Wako 019-11941 Active Carbon-impregnated Silica Gel

【產品名稱】Active Carbon-impregnated Silica Gel?活性炭埋藏硅膠

【制造商】Wako Pure Chemical Industries, Ltd.

【銷售商代碼】019-11941

【規格】10g

【保存條件】Keep at RT.

【外觀】Blackish gray – black, granules – small granules

【注意事項】This product is for research use only. Do not administer it to human.

【?用途】for Dioxins Analysis

活性炭充填硅膠 | 019-11941 【二惡英分析專用】,上海金畔現貨提供?；钚蕴砍涮罟枘z 019-11941。本產品僅用于研究用途。不得用于人體。用于二惡英分析中的預處理（凈化）！活性炭充填硅膠是一種柱凈化填料, 用于微量分析多氯二苯并對二惡英（PCDDs）和多氯二苯并呋喃（PCDFs）。

活性炭充填硅膠?019-11941
本產品僅用于研究用途。不得用于人體。
用于二惡英分析中的預處理（凈化）！
10g包裝
室溫保存

活性炭充填硅膠是一種柱凈化填料,?用于微量分析多氯二苯并對二惡英（PCDDs）和多氯二苯并呋喃（PCDFs）。微量分析要達到高精度要求，就少不了優異的樣品凈化方法。由于二惡英毒性特別高，引起社會廣泛關注，因此進行二惡英分析時，安全性必須十分可靠?；钚蕴烤?有特異吸附具有平板結構的化合物的特性，譬如二惡英?；钚蕴績艋诰聘患河悠肥潜夭豢缮俚倪^程，這點得到全球廣泛認可。然而，傳統的活性炭顆粒存在這樣的弱點：
當顆粒較小時，滲透率較低，而顆粒較大時，在洗脫時會引起嚴重的拖尾現象。
該新型色譜柱填料，采用活性炭充填入硅膠而成，不僅具有活性炭的優良特性，而且具備很好的滲透性。

?活性炭充填硅膠?019-11941 ??[操作程序]

將玻璃棉放在色譜柱的底部，與一個旋塞相連接，加入高度約1厘米的無水硫酸鈉。然后加入1g活性炭充填硅膠，輕輕晃動柱子以使厚度均勻。在頂部再次加入另一層的無水硫酸鈉，高度約0.5厘米。（參考設備圖。）
當柱子裝填完畢，馬上用吸管將樣品（需將正己烷溶液濃縮至0.3毫升左右）慢慢滴加到無水硫酸鈉層上。然后用0.1毫升的正己烷數次洗滌管壁和無水硫酸鈉層。
靜置幾分鐘后，在色譜柱上方連接一個裝有200毫升25%[?v/v]的二氯甲烷/正己烷混合物的分液漏斗，輕輕讓混合液緩緩流下來，開始以每秒鐘1滴的速度進行洗脫。（該洗脫液不含二惡英。）
當二氯甲烷/正己烷混合液加完，繼續用200?mL甲苯以每秒1滴的流速進行洗脫。（該洗脫液含有二惡英。）
將甲苯洗脫液用減壓KD濃縮器濃縮至目標體積。
活性炭充填硅膠?019-11941
[注意事項]
多氯聯苯可以用25%二氯甲烷/正己烷完全洗脫出來，用于定量分析。
由于采用的是干燥型柱層析，在洗脫過程中，氣泡會留在柱內。不過對于回收率和重現性無不良影響。
當1,2,3,4-T4CDD?和O8CDD單組份荷載為1ng時，回收率超過90%。
T4CDD?:?Tetrachlorodibenzo-p-dioxin?四氯二苯并-對-二惡英
O8CDD?:?Octachlorodibenzo-p-dioxin?八氯二苯并-對-二惡英

活性炭充填硅膠?019-11941 ?【參考文獻】

M. Ono, T. Wakimoto, R. Tatsukawa, Y. Masuda, Chemosphere, 15, 1629 (1986)
「日本分析化學會第34年會講演要旨集」p.402 (1985)

貨號???品名?????規格? Cas

012-01965?? Alminium Oxide?? 500g???? –

012-03305?? Ammonium Dihydrogenphosphate? 500g???? 7722-76-1

012-08643?? Amino Acids Mixture Standard Solution, Type B 1mL×5A –

013-08391?? Amino Acids Mixture Standard Solution, Type H 5mL????? –

015-14461?? Amino Acids Mixture Standard Solution, Type AN-2? 5mL????? –

Wako 019-11941 Active Carbon-impregnated Silica Gel?現貨

015-25191?? Anti Phosphorylated α-Synuclein, Monoclonal Antibody (pSyn#64)????? 50ul????? –

011-14463?? Amino Acids Mixture Standard Solution, Type AN-2? 1mL×5A –

011-19365?? 2,2′-Azobis[2-(2-imidazolin-2-yl)propane]

Dihydrochloride?? 500g???? 27776-21-2

016-08641?? Amino Acids Mixture Standard Solution, Type B 5mL????? –

016-20001?? Anti Iba1, Rabbit (for Western Blotting) ??? 50μg???? –

016-23281?? Anti Rat P2X4, Monoclonal Antibody???? 50ug???? –

017-19362?? 2,2′-Azobis[2-(2-imidazolin-2-yl)propane] Dihydrochloride ?? 25g 27776-21-2

018-08721?? Agar, Powder???? 100g???? 9002-18-0

018-22021?? Anti Mouse Ago2, Monoclonal Antibody 100μL??? –
019-03435?? Ammonium sulfate??? 500g???? 7783-20-2

019-19741?? Anti Iba1, Rabbit (for Immunocytochemistry)??? 50μg???? –

019-22291?? Anti Olfactory Marker Protein, Goat????? 100μL??? –

021-02195?? Boric acid???? 500g???? 10043-35-3

021-16201?? BES-H2O2(Cell-impermeant)?? 1mg????? –

031-17601?? Collagenase Type I??? 100mg?? 9001-12-1

032-08385?? Citric Acid Monohydrate?? 500g???? 5949-29-1

032-15372?? Casein Phosphopeptide??? 25g –

034-06363?? N-Caprylic Acid?? 25mL??? 124-07-2

034-16111?? Cefotaxime Sodium Salt?? 1g?? 64485-93-4

035-04595?? Creatinine??? 500g???? 60-27-5

035-17604?? Collagenase Type I??? 1g?? 9001-12-1

038-23221?? α-Casein, from Bovine Milk, Dephosphorylated? 1mg????? –

039-01335?? Carboxymethyl Cellulose Sodium Salt ? 500g???? 9004-32-4

021-17801?? BES-So-AM 1mg????? 936356-51-3

022-07985?? γ-Butyrolactone? 500mL?? 96-48-0

025-03195?? Buffer Solution Standard (Phosphate pH Standard Equimolal Solution)

pH6.86 (25 degrees C)??? 500mL?? –

047-18863?? Dexamethasone 100mg?? 50-02-2

049-18801?? 4′,6-Diamidino-2-phenylindole Dihydrochloride n-Hydrate????? 10mg????? 28718-90-3

058-07681?? EasySeparator??? 1set????? –

025-03195?? Buffer Solution Standard (Phosphate pH Standard Equimolal Solution)

Wako 019-11941 Active Carbon-impregnated Silica Gel?現貨

pH6.86 (25 degrees C)??? 500mL?? –

019-08393?? Amino Acids Mixture Standard Solution, Type H 5Ax1mL –

019-11941?? Active Carbon-impregnated Silica Gel ? 10g –

019-19741?? Anti Iba1, Rabbit (for Immunocytochemistry)??? 50μg???? –

025-15481?? BES-Thio???? 1mg????? –

026-16371?? BF-170? 1mg????? –

027-01276?? Benzyl Alcohol??? 500mL?? 100-51-6

028-03185?? Buffer Solution Standard (Phthalate pH Standard Solution)

pH4.01 (25 degrees C)??? 500mL?? –

028-03185?? Buffer Solution Standard (Phthalate pH Standard Solution)

pH4.01 (25 degrees C)??? 500mL?? –

028-03205?? Buffer Solution Standard (Tetraborate pH Standard Solution)

pH9.18 (25 degrees C)??? 500mL?? –

077-03155?? Gelatin?? 500g???? 9000-70-8

081-00136?? Heparin Sodium? 10mu??? 9041-08-1

088-00705?? L-Histidine Hydrochloride Monohydrate ???? 500g???? 5934-29-2

093-06471?? Insulin, Human, recombinant?? 50mg??? –

097-06474?? Insulin, Human, recombinant?? 1g?? 11061-68-0

120-04891?? L-012??? 100mg?? –

125-05061?? Lysyl Endopeptidase, Mass Spectrometry Grade ???? 5×20μg? –

Wako 019-11941 Active Carbon-impregnated Silica Gel?現貨

125-05061?? Lysyl Endopeptidase, Mass Spectrometry Grade ???? 5×20μg? –

129-02541?? Lysyl Endopeptidase( R)?? 10AU???? –

129-04861?? LY 294002?? 5mg????? 154447-36-6

130-07871?? Melibiose???? 5g?? 585-99-9

028-16211?? BES-So (Cell-impermeant)????? 1mg????? –

028-17811?? BES-H2O2-Ac???? 1mg????? –

029-16361?? BF-168? 1mg????? –

039-23511?? CultureSure? Freezing Medium??? 100ml??? –

041-18861?? Dexamethasine?? 1g?? 50-02-2

042-29445?? Dibasic Sodium Phosphate Hydrate 500g???? 10039-32-4

043-22611?? Dextran 200,000 100g???? 9004-54-0

064-05381?? Fibroblast Growth Factor (basic)(FGFb / bFGF / FGF2),

Human, recombinant, Animal-derived-free? 50ug???? 106096-93-9

071-02293?? gamma-Globulin, from Human Serum?? 5g?? 9007-83-4

075-03075?? Gellan Gum? 500g???? 71010-52-1

131-00405?? Magnesium Sulfate??? 500g???? 10034-, 99-8

136-03032?? Methyl Red?? 25g 493-52-7

137-06085?? Molecular Sieves 4A1/16? 500g???? 70955-01-0

138-07872?? Melibiose???? 25g 585-99-9

145-08221?? Nuclease P1 500u???? 54576-84-0

162-09115?? Polyethylene Glycol 4,000 500g???? 25322-68-3

163-03545?? Potassium Chloride??? 500g???? 7447-40-7

164-21655?? N/400 Potassium Polyvinyl Sulfate Solu 500mL?? 26837-42-3

191-01785?? Trisodium Citrate Dihydrate??? 500g???? 6132-04-3

193-02041?? Glycerol 2-Phosphate Disodium Salt n-Hydrate?? 100g???? 819-83-0

195-12854?? Streptavidin, from Streptomyces avidinii???? 5mg????? 9013-20-1

195-16031?? StemSure (R) Freezing Medium???? 100ml??? –

196-00015?? Sucrose 500g???? 57-50-1

196-08675?? Sodium Dodecyl Sulfate??? 500g???? 151-21-3

197-07485?? Sodium Sulfate?? 500g???? 7757-82-6

199-02825?? Sodium Dihydrogenphosphate Dihydrate ?? 500g???? 13472-35-0

203-17561?? Trichostatin A???? 1mg????? 58880-19-6

207-00055?? L(+)-Tartaric Acid???? 500g???? 87-69-4

208-08385?? 1mol/l Triethylammonium Hydrogencarbonate Solution?? 500mL?? 15715-58-9

223-02112?? VA-044? 25g 27776-21-2

225-02111?? VA-044? 100g???? 27776-21-2

165-09105?? Polyethylene Glycol 2,000 500g???? 25322-68-3

165-17035?? Polyvinylpyrrolidone K 30 500g???? 9003-39-8

167-09045?? Polyethylene Glycol 200?? 500g???? 25322-68-3

169-04245?? Potassium Dihydrogen Phosphate? 500g???? 7778-77-0

169-09125?? Polyethylene Glycol 6,000 500g???? 25322-68-3

185-01003?? Rifampicin??? 5g?? 13292-46-1

186-01114?? all-trans-Retinoic Acid 50mg??? 302-79-4

189-01001?? Rifampicin??? 1g?? 13292-46-1

190-05535?? Trisodium Citrate Dihydrate??? 500g???? 6132-04-3

191-01665?? Sodium Chloride? 500g???? 7647-14-5

227-01071?? Valproic Acid 5g?? 99-66-1

231-02011?? Wetting Tension Test Mixture No.52.0? 50mL??? –

232-01941?? Wetting Tension Test Mixture No.42.0? 50mL??? –

233-01971?? Wetting Tension Test Mixture No.45.0? 50mL??? –

234-02001?? Wetting Tension Test Mixture No.50.0? 50mL??? –

235-01931?? Wetting Tension Test Mixture No.41.0? 50mL??? –

235-02031?? Wetting Tension Test Mixture No.56.0? 50mL??? –

236-01961?? Wetting Tension Test Mixture No.44.0? 50mL??? –

238-01921?? Wetting Tension Test Mixture No.40.0? 50mL??? –

238-02021?? Wetting Tension Test Mixture No.54.0? 50mL??? –

238-02141?? Wetting Tension Test Mixture No.73.0? 50mL??? 7732-18-5

253-00513?? Y-27632 5mg????? 331752-47-7

257-00511?? Y-27632 1mg????? 331752-47-7

290-34251?? Presep-C DNPH?? 20EA???? –

296-63801?? LabAssay? Phospholipid?? 1300tests???? –

298-64101?? Fructooligosaccharides standard set???? set? –

302-93561?? Phos-tag (TM) Agarose??? 0.5mL??? –

304-93521?? Phos-tag (TM) Acrylamide AAL-107????? 10mg??? –

290-34251?? Presep-C DNPH?? 20EA???? –

290-63701?? LabAssay? Triglyceride??? 1000tests???? -2016-2-29

290-65901?? LabAssay? Creatinine????? 500tests –

291-58601?? Lab Assay ALP??? 900tests –

293-51601?? Endotoxin Extracting Solution for LAL Test? 10mL x 4???? –

294-62001?? DsDD cDNA Subtraction kit Wako?? 5tests??? –

294-63601?? LabAssay? NEFA 750tests –

294-65801?? LabAssay? Cholesterol ?? 1000tests???? –

295-50201?? DNA Extractor? Kit?? 50tests? –

295-51301?? Limulus ES-II Single Test Wako???? 25 tests –

295-73401?? Fructooligosaccharides Set????? Set? –

304-93526?? Phos-tag (TM) Acrylamide AAL-107 5mM Aqueous Solution?? 0.3ml??? –

305-93551?? Phos-tag? Mass Analytical Kit set? –

308-93541?? Phos-tag (TM) Biotin BTL-105 10mg??? –

308-93563?? Phos-tag (TM) Agarose??? 3mL????? –

308-97201?? Phos-tag Biotin BTL-1111 1mM Aqueous Solution??? 0.1000mL??? –

325-88521?? Lipase PS Amano SD? 10g –

298-65701?? LabAssay? Glucose?? 1000tests???? –

300-93523?? Phos-tag (TM) Acrylamide AAL-107????? 2mg????? –

301-93531?? Phos-tag (TM) Biotin BTL-104 10mg??? –

301-99413?? Phos-tagTM Biotin BTL-104 1mM Aqueous Solution[for Campaign]???? 0.1mL????? 753451-66-0

302-93522?? Phos-tagTM Acrylamide AAL-107 5mM Aqueous Solution[for Campaign]????? 0.3mL??? 871839-54-2

631-00651?? Cellmatrix Type I -A (Collagen, Type I, 3 mg/mL, pH 3.0)???? 20mL??? –

637-00653?? Cellmatrix Type I -A (Collagen, Type I, 3 mg/mL, pH 3.0)???? 100mL?? –

638-01021?? Endotoxin Standad /JPSE? 10000un????? –

986-10001?? Anti asialo GM1 (Rabbit), (014-09801)? 1mL ???? 617-45-8

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Wako 019-11941 Active Carbon-impregnated Silica Gel